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黄剑锋, 羊俊, 贺海燕, 吴建鹏. X射线衍射物相定量分析内标法标准曲线库的建立[J]. 岩矿测试, 2006, 25(3): 215-218.
引用本文: 黄剑锋, 羊俊, 贺海燕, 吴建鹏. X射线衍射物相定量分析内标法标准曲线库的建立[J]. 岩矿测试, 2006, 25(3): 215-218.
Development and Application of a Standard Curve Database in Quantitative Phase Analysis by XRD Based on the Internal Standard Method[J]. Rock and Mineral Analysis, 2006, 25(3): 215-218.
Citation: Development and Application of a Standard Curve Database in Quantitative Phase Analysis by XRD Based on the Internal Standard Method[J]. Rock and Mineral Analysis, 2006, 25(3): 215-218.

X射线衍射物相定量分析内标法标准曲线库的建立

Development and Application of a Standard Curve Database in Quantitative Phase Analysis by XRD Based on the Internal Standard Method

  • 摘要: 在Rigaku D/Max-2200型X射线衍射仪(XRD)定量分析软件的基础上,制作了无机非金属材料中常用的SiO2(石英)、Al2O3(刚玉)、TiO2等9种组分用XRD采用内标法进行物相定量分析时的标准曲线。结果表明,这些标准曲线的可信度R在0.928~0.980。通过对已知含量样品的测量,分析结果与实际值一致,说明建立的标准曲线完全可用于高精度物相定量分析。

     

    Abstract: Based on the quantitative analysis software attached in Rigaku D/Max-2200 X-ray diffractometer, a standard curve database for quantitative phase analysis by XRD with internal standard method for 9 inorganic compounds including quartz, corundum, TiO2, etc.

     

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