准噶尔盆地西北部风城组页岩油微观赋存特征及甜点预测

Microscopic Occurrence Characteristics and Sweet Spot Prediction of Shale Oil in Fengcheng Formation, Northwest Junggar Basin

  • 摘要: 准噶尔盆地西北部风城组是盆地的主力烃源岩,是未来页岩油勘探开发的重点层位。前人研究主要针对风城组的沉积环境、岩石学、储层孔隙结构及物性等方面,但对于页岩油微观赋存特征相关研究较为薄弱。为揭示准噶尔盆地西北部风城组不同岩相页岩的含油性与页岩油微观赋存特征,本文采集4口钻井的81件泥页岩样品,通过场发射扫描电子显微镜(FE-SEM)、核磁共振(NMR)、分步抽取实验联合应用,建立了一种研究复杂岩相页岩油赋存状态影响因素的方法,有效避免了单项实验带来的误差及偶然性,系统表征研究区6种岩相页岩油赋存特征。实验证实,FE-SEM与NMR的联合应用,能有效识别页岩油赋存状态,游离油表现为T2>2ms、T1/T2≈10的线性分布,主要赋存于>50nm的孔隙和微裂缝中,吸附油表现为T2<2ms、T1/T2≈100的带状分布,主要以油膜形式存在于黏土矿物表面及黄铁矿集合体内,可为区分页岩油的甜点岩相提供技术支撑;NMR测试方法与轻重烃三次分步抽取实验的联合应用,并结合不同岩相页岩油储集类型发育特征,明确指出灰质泥页岩为研究区风城组最有利岩相,其次为白云质泥页岩(赋油能力最强)和白云质凝灰岩。其中,哈深斜1井区风三段具有高含油性(TOC 1.5%~5.13%,S1 1.2~4.02mg/g,游离油占比20%~40%),高孔隙度(孔隙度4.2%~6.58%,发育粒内孔、粒间孔和微裂缝),高脆性(脆性矿物含量55%~71%,里氏硬度450~650,可压性好)等特征,为最有利目标层段。

     

    Abstract: The Fengcheng Formation (P1f) is the main source rock in the northwest Junggar Basin, and is the key horizon for shale oil exploration and development in the future. Previous studies mainly focus on the sedimentary environment, petrology, reservoir pore structure and physical properties of P1f but the relevant research on the microscopic occurrence characteristics of shale oil is relatively weak. To reveal the oil content and micro-occurrence characteristics of shale oil in different lithofacies of P1f in northwest Junggar Basin, this paper used 81 mud/shale samples from 4 wells to effectively avoid the errors and accidents caused by single experiments through the joint application of field emission scanning electron microscope (FE-SEM), nuclear magnetic resonance (NMR) and stepwise extraction experiments. And systematically characterizes the occurrence state across six lithofacies of shale oil in the study area. The experimental results show that the combined application of SEM and NMR method can effectively identify shale oil occurrence states. Free oil exhibits a linear distribution of T2>2ms, T1/T2≈10, mainly residing in pores and microfractures >50nm. Adsorbed oil shows a zonal distribution of T2<2ms and T1/T2≈100, occurring as oil films on clay mineral surfaces and within pyrite aggregates. These findings can provide technical support for distinguishing sweet spot shale oil. Combined with the application of NMR method and three-step light/heavy hydrocarbon extraction, and combined with the development characteristics of different lithofacies of shale oil reservoirs, it is clearly pointed out that the calcareous mudstone/shale is the most favorable lithofacies of P1f, in the study area, followed by dolomitic mudstone/shale (with the strongest oil capacity) and the dolomitic tuff, Among them, the third member of P1f in the area of Well Hashenxie 1 has high oil content (TOC 1.5%-5.13%, S1 1.2-4.02mg/g, free oil accounting for 20%-40%), high porosity (porosity 4.2%-6.58%, development of intragranular pores, intergranular pores and micro-fractures), high fracability (brittle mineral content 55%-71%, hardness 450-650, good compressibility) and other characteristics, which are the most favorable target section.

     

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