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王羽, 汪丽华, 王建强, 王彦飞. 利用微米X射线显微镜研究陆相延长组页岩孔隙结构特征[J]. 岩矿测试, 2020, 39(4): 566-577. DOI: 10.15898/j.cnki.11-2131/td.202003110030
引用本文: 王羽, 汪丽华, 王建强, 王彦飞. 利用微米X射线显微镜研究陆相延长组页岩孔隙结构特征[J]. 岩矿测试, 2020, 39(4): 566-577. DOI: 10.15898/j.cnki.11-2131/td.202003110030
WANG Yu, WANG Li-hua, WANG Jian-qiang, WANG Yan-fei. Investigation on Pore Structures of Yanchang Formation Shale Using Micro X-ray Microscopy[J]. Rock and Mineral Analysis, 2020, 39(4): 566-577. DOI: 10.15898/j.cnki.11-2131/td.202003110030
Citation: WANG Yu, WANG Li-hua, WANG Jian-qiang, WANG Yan-fei. Investigation on Pore Structures of Yanchang Formation Shale Using Micro X-ray Microscopy[J]. Rock and Mineral Analysis, 2020, 39(4): 566-577. DOI: 10.15898/j.cnki.11-2131/td.202003110030

利用微米X射线显微镜研究陆相延长组页岩孔隙结构特征

Investigation on Pore Structures of Yanchang Formation Shale Using Micro X-ray Microscopy

  • 摘要: 页岩孔隙结构是决定储层储集与运移能力的关键,对完善我国陆相页岩气产能评估方法和压裂技术具有重要意义。本文选取鄂尔多斯盆地陆相延长组7段页岩,利用氩离子抛光-扫描电镜和微米X射线显微镜方法研究其孔隙结构特征与三维空间分布特征。扫描电镜结果表明,延长7段页岩中主要发育粒间孔(300~600nm)和微裂缝,是页岩气的主要储集空间。微裂缝多由黏土矿物沉淀形成,以平直状为主,易引发井壁坍塌等严重问题。有机孔发育较少,一般与有机黏土矿物共存,绝大部分有机质呈致密状。微米X射线显微镜测试进一步表明,长7段页岩在三维空间具有微米级纹层结构,其中有机质纹层厚10~20μm,揭示了延长组7段页岩层具有较强塑性,不利于水平压裂。该研究成果将为构建延长7段页岩气渗流模型、改进压裂技术提供重要数据支持。

     

    Abstract:
    BACKGROUNDShale pore structure is the key to determine reservoir storage and migration capacity. It is of great significance for improving the productivity assessment of continental shale gas in China, and fracturing technology.
    OBJECTIVESTo investigate the pore structure and three dimensional distribution mode of the seventh member of Yanchang Formation shale and its controlling factors.
    METHODSAr-ion milling SEM and synchrotron micro X-ray microscopy were used to characterize the pore structures.
    RESULTSThe SEM results indicated that the interparticle pores (300-600nm) and micro-fractures were the main reservoir space of the seventh member of Yanchang Formation shale gas. Most of the micro-fractures were formed by the precipitation of clay minerals and presented as a flat shape, which likely caused collapse of borehole walls. Organic pores were less developed and mainly associated with organic clay minerals. The micro X-ray microscopy showed that the seventh member of Yanchang Formation shale had laminated structures at micro-scale with organic matter laminations of 10-20μm in thickness. The results indicated that the seventh member shale had strong plasticity, which was against horizontal fracturing.
    CONCLUSIONSThe results can provide significant data support for developing a percolation model and improving fracturing technology of shale gas.

     

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